TIMEleSS Tools for Multigrain X-ray Diffraction

TIMEleSS toolsIn addition to contributing the TIMEleSS Multigrain Wiki, TIMEleSS members also released a set of python and matlab utilities to process, analyze, plot, and understand multigrain X-ray diffraction data. All are released under an open-source licence at GitHub on the TIMEleSS-tools and TIMEleSS-Matlab repositories.

TIMEleSS-tools include various utilities to process images, clean up parasite signals on the X-ray diffraction images, manage your peaks and grains, and post-process the output of the various multigrain XRD sofwares.

TIMEleSS-Matlab are MTEX functions one can use to represent grain orientations in pole or inverse pole figures with efficient and intuitive color scales.

Enjoy, and do not hesitate to push any improvement you might make!

TIMEleSS Multigrain Wiki

TIMEleSS Multigrain WikiMultigrain X-ray diffraction (sometimes called 3D-XRD or HEDM depending on communities) allows characterizing hundreds of crystals in a polycrystalline material. It has been adapted to diamond anvil cell experiments for the investigation of materials under high pressure and high temperature. The method lies at the core of the experimental portion of the TIMEleSS project. We use it to characterize transformation and deformation microstructures in mantle minerals.

Multigrain X-ray diffraction can be hard to learn and implement. Hence, along the course of the project, timeless members documented their procedures for processing such data in an online documentation: the TIMEleSS Multigrain Wiki.

We are now finished with our rounds of experiments, data has been processed, and results are being submitted for publication, so it is time to give back to the community! The TIMEleSS Multigrain Wiki has been accessible for years to who knew the URL. Now the link is public and should be easy to find with your best search engines. Please use it, enjoy it, and do not hesitate to contact us if you want to contribute and suggest corrections

This wiki, among with other outputs, was used as a basis for the creation of the Commission on Diffraction Microstructure Imaging of the International Union of Crystallography. This new Commission on Diffraction Microstructure Imaging was established at the Prague General Assembly in August 2021 and TIMEleSS PI S. Merkel is one of the founding members for the application.

Datatron for the TIMEleSS project

TIMEleSS May 2019 datatron

The synchrotron guys of the TIMEleSS project met up for a datatron the second week of May 2019. During a TIMEleSS datatron, we all sit in a room and get moving on data processing from our recent synchrotron experiments!

The datatron was attented by M. Krug, E. Ledoux, and J. Gay, PhD students involved in the TIMEleSS project, S. Merkel, the PI for TIMEleSS. We also welcomed 3 guests during this week: J. Wright, from ID11 at ESRF, A. Dewaële from CEA, and M. Bykov from the Bayerisches Geoinstitut.

The next TIMEleSS datatron has not been planned yet but may happen later in 2019.

TIMEleSS PI giving an invited presentation at the Diamond light source

Diamond High-Pressure Workshop, 26/02/2019 - 27/02/2019

S. Merkel gave an invited presentation at the Diamond Light Source workshop on high pressure research, in the UK.

The workshop aims to bring together high-pressure researchers with different experimental expertise and to highlight the latest developments in high-pressure techniques across synchrotron beamlines.

S. Merkel gave a presentation entitled “In situ study of phase transformation mechanisms using multigrain crystallography“. The presentation was an opportunity to present the science at the foundation of the TIMEleSS project, its objectives, and some results.

Second multigrain diffraction training session for TIMEleSS members

Second training session on multigrain analysis, February 2019

The TIMEleSS team is holding its second training session on multigrain diffraction data processing. The session takes place on Feb 11-15 at the Université de Lille, in France. Participants (left to right on the image) include Julien Chantel, our guest Agnès Dewaele, Sébastien Merkel, Jeffrey Gay, Sergio Speziale, Estelle Ledoux, Matthias Krug, and Carmen Sanchez-Valle.

The session is an opportunity for all members to get trained in multigrain diffraction data processing but also to standardize our data workflow strategies.

More to come soon with the TIMEleSS-tools developed at this occasion!

TIMEleSS PI giving invited lecture in Les Houches

CREEP Final Workshop Ecole de Physique des Houches (F) 27 January – 1 February 2019

This week, two of the TIMEleSS PI’s are attenting the Final Workshop of the CREEP ITN at the Ecole de Physique des Houches, in France. The workshop is held from 27 January to 1 February 2019 in the town of Les Houches, in the Chamonix valley.

The CREEP ITN is a EU funded project that proposed an interdisciplinary and multiscale approach to study the origin of rheological complexity in Earth and analogous materials and how it controls the dynamics of our planet, including natural and human-induced seismicity, and affects a large range of industrial applications, from energy production and waste storage to production of high-performance glasses. It included a number of partners, from academia and industry with over 10 PhD fellowships. More details can be seen at the CREEP ITN website.

The TIMEleSS project, its objectives, and some results were highlighted in a an hour long invited presentation regarding Phase transitions in the mantle by PI S. Merkel.

PhD student day in Lille

Jeff Gay and Estelle Ledoux at PhD student days at UMET in Lille in 2019

Estelle Ledoux and Jeff Gay presented they current work at the PhD student days for the UMET lab in Lille. The symposium is organized yearly in January.

This one-day meeting is an opportunity to discover the work of current PhD students and the evolution of research in the lab. It is an opportunity for exchanges between students and researchers, exchange ideas, and build strong future collaborations.

The full program of the symposium can be found online in the following document.

Deep Earth Mini Symposium at WWU Münster

Federica Rochira and Matthias Krug at the Deep Earth Mini Symposium in Münster in December 2018

Federica Rochira and Matthias Krug presented posters at the Deep Earth Mini Symposium in Münster. The symposium was organized by TIMEleSS PI Tine Thomas.

This one-day meeting attracted an international and interdisciplinary group of deep Earth scientists, PhDs and Master students, with keynote talks given by Jennifer Jackson (Caltech), Jeroen Ritsema (University of Michigam) and Sebastian Rost (University of Leeds), and a poster session with wine and cheese.

The full program of the symposium can be found online in the following document.